102T Pharmaceutical Analysis I – Theory

Pharmaceutical Analysis 1 Theory syllabus, Notes, MCQ, PDF

BP102T Pharmaceutical Analysis I – Theory

UNIT-I

(a) Pharmaceutical analysis- Definition and scope

i) Different techniques of analysis

ii) Methods of expressing concentration

iii) Primary and secondary standards.

iv) Preparation and standardization of various molar and normal solutions

Oxalic acid,

Sodium hydroxide,

Hydrochloric acid,

Sodium thiosulphate,

Sulphuric acid,

Potassium permanganate,

Ceric ammonium sulphate

(b)Errors

Sources of errors,

Types of errors,

Methods of minimizing errors,

Accuracy, precision and significant figures

(c)Pharmacopoeia,

Sources of impurities in medicinal agents,

Limit tests.

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UNIT-II

Acid base titration

Theories of acid-base indicators,

Classification of acid-base titrations

Theory involved in titrations of strong, weak, and very weak acids and bases,

Neutralization curves

Non aqueous titration

Solvents,

Acidimetry and alkalimetry titration,

Estimation of Sodium benzoate,

Estimation of Ephedrine HCl

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UNIT-III

Precipitation titrations

Mohr’s method,

Volhard’s, Modified Volhard’s,

Fajans method,

Estimation of sodium chloride

Complexometric titration

Classification,

Metal ion indicators,

Masking and demasking reagents,

Estimation of Magnesium sulphate,

Estimation of calcium gluconate.

Gravimetry

Principle and steps involved in the gravimetric analysis.

Purity of the precipitate: co-precipitation and post precipitation,

Estimation of barium sulphate.

Diazotisation titration.

Basic Principles,

Methods

Application of diazotisation titration.

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UNIT-IV

Redox titrations

(a) Concepts of oxidation and reduction

(b) Types of redox titrations (Principles and applications)
Cerimetry,
Iodimetry,
Iodometry,
Bromatometry,
Dichrometry,
Titration with potassium iodate

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UNIT-V

Electrochemical methods of analysis

Conductometry

Introduction,
Conductivity cell,
Conductometric titrations,
Applications.

Potentiometry

Electrochemical cell,

Construction and working of

Reference electrode
Standard hydrogen electrode,
Silver chloride electrode
Calomel electrode

Indicator electrodes
Metal electrodes
Glass electrode,

Methods to determine endpoint of potentiometric titration

Applications.

Polarography

Principle,

Ilkovic equation,

Construction and working of
Dropping mercury electrode
Rotating platinum electrode,

Applications

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Pharmaceutical Analysis 1 Theory Recommended Books: (Latest Editions)

1. A.H. Beckett & J.B. Stenlake’s, Practical Pharmaceutical Chemistry Vol I & II, Stahlone
   Press of University of London
2. A.I. Vogel, Text Book of Quantitative Inorganic analysis
3. P. Gundu Rao, Inorganic Pharmaceutical Chemistry
4. Bentley and Driver’s Textbook of Pharmaceutical Chemistry
5. John H. Kennedy, Analytical chemistry principles
6. Indian Pharmacopoeia.

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First Year B Pharm Notes, Syllabus, Books, PDF Subjectwise/Topicwise

F Y B Pharm Sem-I	F Y B Pharm Sem-II
BP101T Human Anatomy and Physiology I Theory	BP201T Human Anatomy and Physiology II – Theory
BP102T Pharmaceutical Analysis I Theory	BP202T Pharmaceutical Organic Chemistry I Theory
BP103T Pharmaceutics I Theory	BP203T Biochemistry – Theory
BP104T Pharmaceutical Inorganic Chemistry Theory	BP204T Pathophysiology – Theory
BP105T Communication skills Theory	BP205T Computer Applications in Pharmacy Theory
BP106RBT Remedial Biology	BP206T Environmental sciences – Theory
BP106RMT Remedial Mathematics Theory	BP207P Human Anatomy and Physiology II Practical
BP107P Human Anatomy and Physiology Practical	BP208P Pharmaceutical Organic Chemistry I Practical
BP108P Pharmaceutical Analysis I Practical	BP209P Biochemistry Practical
BP109P Pharmaceutics I Practical	BP210P Computer Applications in Pharmacy Practical
BP110P Pharmaceutical Inorganic Chemistry Practical
BP111P Communication skills Practical
BP112RBP Remedial Biology Practical

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